Synthesis of Zn-B-P/Al/Al2o3-Acylation Catalyst Diethylamino M-Toluic Acid under Exposure to Radiation of Microwave Range

P.A. Muradova, V.F. Tretyakov, S.M. Zulfugarova, R.M. Talishinskiy, Yu.N. Litvishkov

The paper presents the results of microwave synthesis of an active energy absorbing microwave radia-tion Zn-B-P-oxide catalyst supported on the surface of the fiber reinforced aluminum Al/γ-Al₂O₃-carrier to further intensification of the process of acylation diethylamine m-toluic acid diethylamide, m-toluic acid (DETA ) under the effect of the microwave field. Established the identity of the phase composition of the active mass of the samples formed un-der the action of microwave radiation (2450MHz) with the phase of the catalyst composition prepared by conventional heat treatment, which considering their more developed active surface also gives rea-son to expect a manifestation of higher catalytic efficiency.